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农业农村部 规范禁养区划定实施方案

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发布时间:2019-10-23 09:35

RUGUONINZHENGZAIXUNZHAOXIANGGUANCHANPINHUOYOUQITARENHEWENTI,KESUISHIBODAGONGSIFUWUREXIAN,HUODIANJIXIAFANGANNIUYUWOMENZAIXIANJIAOLIU!

服务热线:19939951369拨打电话



       用不含二氧化碳的水溶解,移人250ml容量瓶中,稀释至刻度,摇匀。若稀释液深浊,用中速滤纸干过滤,此为试液A.称取约8g液体试样或2.5g固体试样,精确至0. 002g。用移液管移取10ml稀释液或干过滤溶液,置于250ml锥形瓶中,加10ml硝酸溶液,煮沸1min,冷却至室温后加20.00ml乙二胺四乙酸二钠溶液,加百里酚蓝溶液3-4滴,用氨水溶液中和至试液从红色到黄色,煮沸2min,冷却后加入10ml乙酸-乙酸钠缓冲溶液和2~4滴二甲酚橙指示溶液,用氯化锌标准滴定溶液滴定至溶液由淡黄色变为微红色即为终点,同时做空白试验.

YIZHILIANGBAIFENSHUBIAOSHIDEYANGHUALV(Al 0,)HANLIANG(Xi)ANSHI(1)JISUAN:m1.4 FENXIJIEGUODEBIAOSHUXi (%)-(FU V) cX 0.05098 100-(Vo-V) cx127.5SHIZHONG, V。WEIKONGBAISHIYANXIAOHAODELVHUAXINBIAOZHUNDIDINGRONGYEDETIJI, ml; VWEICEDINGSHIYANGDIDINGXIAOHAODELVHUAXINBIAOZHUNDIDINGRONGYEDETIJI, ml; cWEILVHUAXINBIAOZHUNDIDINGRONGYEDESHIJINONGDU, mo/L; mWEISHILIAODEZHILIANG, g: 0.05098WEIYU1.00mlLVHUAXINBIAOZHUNDIDINGRONGYE[c(ZnCl2)=1. 000mo/L]XIANGDANGDEYIKEBIAOSHIDEYANGHUALVDEZHILIANG。

澳门网上葡京真人2.2.2QINGYANGHUANABIAOZHUNDIDINGRONGYE: (NaOH)YUE0.5mol/L2.2.3 FENTAIZHISHIYE: 10g/LYICHUNRONGYE。

澳门网上葡京真人2.2.4 LVHUAJIARONGYE: 250g/L.CHENGQU250gFUHUAJIA,YI200mlBUHANERYANGHUATANDEZHENGLIUSHUIRONGJIEHOU,XISHIZHI1000ml,JIARU2DIFENXIANZHISHIYEBINGYONGQINGYANGHUANARONGYEHUOYANSUANRONGYEDIAOJIERONGYECHENGWEIHONGSE,LVQUBURONGWUHOUZHUYUSULIAOPINGZHONG。

2.3 FENXIBUZHOU

YIQU25. 00mlSHIYEA,ZHIYU250mlMOKOUPINGZHONG,JIA20. 00mlYANSUANBIAOZHUNRONGYE,JIESHANGMOKOUHAILILENGNINGGUAN,ZHUFEIHUILIU2min,LENGQUEZHISHIWEN。ZHUANYIZHIJUYIXIBEIZHONG,JIARU20mlFUHUAJIARONGYE,BAOYUN。JIARU5DIFENTAIZHISHIYE,LIJIYONGQINGYANGHUANABIAOZHUNDIDINGRONGYEDIDINGZHIRONGYECHENGXIANWEIHONGSEJIWEIZHONGDIAN。TONGSHIYONGBUHANERYANGHUATANDEZHENGLIUSHUIZUOKONGBAISHIYAN。SHIZHONG, VoWEIKONGBAISHIYANXIAOHAOQINGYANGHUANABIAOZHUNDIDINGRONGYEDETIJI, ml; VWEICEDINGSHIYANGXIAOHAOQINGYANGHUANABIAOZHUNDIDINGRONGYEDETIJI, ml; cWEIQINGYANGHUANABIAOZHUNDIDINGRONGYEDESHIJINONGDU, mol/L; mWEISHILIAODEZHILIANG, g; XWEI1.4ZHONGCEDEDEYANGHUALVHANLIANG, %; 0. 01699WEIYU1.00mlQINGYANGHUANABIAOZHUNDIDINGRONGYE[c(NaOH) =1. 000mol/L]XIANGDANGDEYIKEBIAOSHIDE[OH-]DEZHILIANG; 0.5293WEIAl:O3ZHESUANCHENGJIANGYETIJULVHUALVSHIYANGZHURUQINGJIE、GANZAODELIANGJIANNEI,BUDEYOUQIPAO。JIANGLIANGJIANZHIYU(20±1)℃DEHENGWENSHUIYUZHONG,DAIWENDUHENGDINGHOU,JIANGMIDUJIHUANHUANFANGRUSHIYANGZHONG。DAIMIDUJIZAISHIYANGZHONGWENDINGHOU,DUCHUMIDUJIWANYUEMIANXIAYUANDEKEDU(BIAOYOUWANYUEMIANSHANGYUANKEDUDEMIDUJICHUWAI),JIWEI20℃SHISHIYANGDEMIDU。

CHENGQUYUE10gYETISHIYANGHUOYUE3gGUTISHIYANG,JINGQUEZHI0.001g,ZHIYU1000mlSHAOBEIZHONG,JIARU500mlSHUI,CHONGFENJIAOBAN,SHISHIYANGRONGJIE。RANHOU,ZAIBUSHILOUDOUZHONG,YONGHENGLIANGDEZHONGSUDINGLIANGLVZHICHOULV。XIZHIWUCI-SHI(YONGXIAOSUANYINRONGYEJIANYAN),JIANGLVZHILIANTONGLV,YU100~105℃GANZAOZHIHENGLIANG。HUOYIDENGYUANSHUICHENGYIZHILIANGBAIFENSHUBIAOSHIDESHUIBURONGWUHANLIANG(X)ANSHI(3)JISUAN:nxs (%) = M-mx100MI

6.1 FANGFATIYAO

SHIYANGZHONGJIARUTANSUANNARONGYESHIAI3+XINGCHENGQINGYANGHUAWUCHENDIAN,YUCHENDIANSHANGQINGYEZHONGJIARUCILVSUANNAHE1CHAFEN,XINGCHENGLANLVSEXUANFENLUOHEWU,ZAIBOZHANG720nmCHUCEDINGQIXIGUANGDU,QIUCHUANTAIDANHANLIANG。

澳门网上葡京真人YONGYIYEGUANYIQU50mlANTAIDANBIAOZHUNZHUBEIRONGYE,YIRU1000mlRONGLIANGPINGZHONG,YONGWUANZHENGLIUSHUIXISHIZHIKEDU,YAOYUN。CIRONGYEXIANPEIXIANYONGZHUYEteFENBIEYIQU0.00, 1.00ml、 2.00ml, 3.00ml、 4.00ml、 5.00ml, 6. 00ml、 7.00mlANTAIDANBIAOZHUNRONGYE,YIRU100mlRONGLIANGPINGZHONG,JIAWUANZHENGLIUSHUIYUE50ml,JIARU1mlCILVSUANNARONGYE,YAOYUN,2~5minNEIJIARU1ml EDTA.QINGYANGHUANAHUNHEYE,YAOYUN,ZAIZAI1~5minNEIJIARU5ml 1-NAIFENRONGYEBINGZAICIYAOYUN,JIASHUIXISHIZHIKEDU,YU25~30℃JINGZHI15min,YONG1cmBISEm,ZAIBO720nmCHUYISHIJIKONGBAIYANGWEICANBICEQIXIGUANGDU。YIANTAIDANDE(mg)SHUWEIHENGZUOBIAO,XIGUANGDUWEIZONGZUOBIAOHUIZHIBIAOZHUNQUXIANCEDINGCHENGQUYUE10gYETISHIYANGHUO3.3gGUTISHIYANG,JINGQUEZHI0.00g。YIRU500mlRONGLIANGPINGZHONG,YONGSHUIXISHIZHIKEDU,YAOYUN。YONGYIYEGUANYIQU25mlCIRONGYE,ZHIYU100mlRONGLIANGPINGZHONG,JIA1. 5mlLIUSUANRONGYEYAOYUNHOU,JIARU5mlTANSUANNARONGYEBINGXISHIZHIKEDU,QINGQINGYAOYUN。JINGZHISHIQINGYANGHUAWUCHENDIAN。YONGYIYEGUANYIQU50mlSHANGQINGYEYU100mlRONGLIANGPINGZHONG,YONGQINGYANGHUANARONGYEDIAOpHZHIZHIYUE11。YIXIAANHUIZHIBIAOZHUNQUXIANBUZHOUJINXINGXIGUANGDUDECEDING。SHIZHONG, mWEICONGQUXIANSHANGDEDAODEANTAIDAN(N)DEZHILIANG, mg: moWEISHILIAODEZHILIANG。JULIUSUANTIECHANPINANYONGTUFENWEILIANGLEI。1LEI:YINYONGSHUIYONG;1LEI:GONGYEYONGSHUI、WUSHUIYONG。WAIGUAN:TIWEIHONGHESENIANCHOUTOUMINGYETI;GUTIWEIDANHUANGSEWUDINGXINGGUTI。JULIUSUANTIEZHIBIAOYINGFUHEBIAO2YAOQIU。JIANGJULIUSUANTIESHIYANG(1XING)ZHURUQINGJIE、GANZAODELIANGJIANNEI,BUDEYOUQIPAO。JIANGLIANGJIANZHIYU(201)℃DEHENGWENSHUIYUZHONG,DAIWENDUHENGDINGHOU,JIANGMIDUJIHUANHUANDIFANGRENSHIYANGZHONG,DAIMIDUJIZAISHIYANGZHONGWENDINGHOU,DUCHUMIDUJIWANYUEMIANXIAYUANDEKEDU(BIAOYOUDUWANYUEMIANSHANGYUANDEKEDUDEMIDUJICHUWAI),JIWEI20℃SHIYANGDEMIDU。

2.1.1 FANGFATIYAO

ZAISUANXINGRONGYEZHONG,DIJIASANLVHUATAIRONGYEJIANGSANJIATIELIZIHAIYUANWEIERJIA,GUOLIANGDESANLVHUATAIJINYIBUJIANGWUSUANNAZHISHIYEHAIYUANSHENGCHENG“WULAN”,SHIRONGYECHENGLANSE。ZAIYOUTONGYANDECUIHUAXIA,JIEZHUSHUIZHONGDERONGJIEYANGYANGHUAGUOLIANGDESANLVHUATAI,DAIRONGYEDELANSEXIAOSHIHOU,JIYIERBENANHUANGSUANNAWEIZHISHIJI,YONGZHONGGESUANJIABIAOZHUNDIDINGRONGYEDIDING。FANYINGFANGCHENGSHIWEI。

澳门网上葡京真人2.1.2.6SANLVHUATAIRONGYE:LIANGQU25ml 15%DESANLVHUATAIRONGYE,JIARU20mlYANSUANRONGYE,YONGSHUIXISHIZHI100ml,HUNYUN,ZHUYUZONGSEPINGZHONG,RONGYESHANGMIANJIAYIBOCENGYETISHILABAOHU,KEYONG15dZUOYOU。2.1.2.5 LIUSUANTONGRONGYE: 5g/L.CHENGQU2.5gWUSUANNA,RONGJIEYU70mlSHUIZHONG,JIARU7mlLINSUANRONGYE,LENGQUEHOUYONGSHUIXISHIZHI10m.2.1.2.7WUSUANNAZHISHIJI: 25g/L.

2. 1.2.8ZHONGGESUANJIABIAOZHUNDIDINGRONGYE: c(1/6k,Cr0n)=0. 1mol/L2.1.2.9ERBENANHUANGSUANNARONGYE: 5g/L.HUNYUN,ZHUYUZONGSEPINGZHONG。

CHENGQUYUE0.2~0.3gSHIYANG(JINGQUEZHI0.00018),ZHIYU250mlZHUIXINGPINGZHONG,JIAYANSUANRONGYE10ml,LIUSUANRONGYE10mlHEWUSUANNAZHISHIJI1ml.ZAIBUDUANYAODONGXIA,ZHUDIJIARUSANLVHUATAIRONGYEZHIZHIRONGYEGANGHAOCHUXIANLANSEWEIZHI。YONGSHUICHONGXIZHUIXINGPINGNEIBI,BINGXISHIZHIYUE150ml,JIARU2DILIUSUANTONGRONGYE,CHONGFENYAODONG,DAIRONGYEDELANSEXIAOSHIHOU,JIARULINSUANRONGYE10mlHE2DIERBENANHUANGSUANNAZHISHIJI,LIJIYONGZHONGGESUANJIABIAOZHUNDIDINGRONGYEDIDINGZHIZISE(30sBUTUN)JIWEIZHONGDIAN。

2.1.4 JIEGUODEBIAOSHU

QUANTIEHANLIANGYIZHILIANGFENSHUW;JI,SHUZHIYI%BIAOSHI,ANSHI(5)JISUAN:W;(%)= cVxo。05585×xlooMISHIZHONG, cWEIZHONGGESUANJIABIAOZHUNDIDINGRONGYENONGDUDEZHUNQUESHUZHI, mol/L, VWEIDIDINGSHIXIAOHAOZHONGGESUANJIABIAOZHUNDIDINGRONGYEDETIJIDESHUZHI, ml 0.055WEIYU1.00mlZHONGGESUANJIABIAOZHUNDIDINGRONGYE[C(1/6KCr20)1.000mol/]XIANGDANGDEYIKEBIAOSHIDETIEDEZHILIANG; mWEISHILIAODEZHILIANGDESHUZHI,。

2.2ZHONGGESUANJIAFA

YETICHANPINCHENGQUYUE(1.50.001)gSHIYANG,GUTICHANPINCHENGQUYUE(0.910.001)gSHIYANG,ZHIYU250mlZHUIXINGPINGZHONG,JIAZHENGLIUSHUI20ml,JIAYANSUANRONGYE20ml,JIAREZHIFEI,CHENREDIJIALVHUAYAXIRONGYEZHIRONGYEHUANGSEXIAOSHI,ZAIGUOLIANG1DI,KUAISULENGQUE,JIALVHUAGONGBAOHERONGYE5ml,YAOYUNHOUJINGZHI1min,RANHOUJIASHUI50ml,ZAIJIARULIULINHUNSUAN10ml,ERBENANHUANGSUANNAZHISHIJI4~5DI,LIJIYONGZHONGGESUANJIABIAOZHUNDIDINGRONGYEDIDINGZHIZISE(30sBUTUN)JIWEIZHONGDIAN。YAOMINHUILIANZHANGSHIZHONG, cWEIZHONGGESUANJIABIAOZHUNDIDINGRONGYENONGDUDEZHUNQUESHUZHI, mol/L; VWEIDIDINGSHIXIAOHAOZHONGGESUANJIABIAOZHUNDIDINGRONGYEDETIJIDESHUZHI, ml; 0.055WEIYU1.00mlZHONGGESUANJIABIAOZHUNDIDINGRONGYE[C(1/6K.Cr20)=1.000mol/]XIANGDANGDEYIKEBIAOSHIDETIEDEZHILIANG; mWEISHILIAODEZHILIANGDESHUZHI。CHENGQUYUE(5±0.001) gSHIYANG,ZHIYU250mlZHUIXINGPINGZHONG,JIASHUI50ml,JIARULIUSUAN4ml,LINSUAN4ml,YAOYUN。YONGGAOMENGSUANJIABIAOZHUNDIDINGRONGYE3.2.4DIDINGZHIWEIHONGSE(30sBUTUN)JIWEIZHONGDIAN,TONGSHIZUOKONGBAISHIYAN。

3.5JIEGUODEBIAOSHU

HAIYUANXINGWUZHI(YIFetJI)HANLIANGYIZHILIANGFENSHUW,JI,SHUZHIYI%BIAOSHI,ANSHI(7)JISUAN:Ws (%) = (V-Vo) cX0.0558×x100MI

澳门网上葡京真人SHIZHONG, cWEIGAOMENGSUANJIABIAOZHUNDIDINGRONGYE3.2. 4NONGDUDEZHUNQUESHUZHI, mol/L, VWEIDIDINGSHIXIAOHAOGAOMENGSUANJIABIAOZHUNDIDINGRONGYEDETIJIDESHUZHI, ml, V。WEIDIDINGKONGBAISHIXIAOHAOGAOMENGSUANJIABIAOZHUNDIDINGRONGYEDETIJIDESHUZHI, ml; 0. 05585WEIYU1.00mlGAOMENGSUANJIABIAOZHUNDIDINGRONGYE[c(1/5KMnO)=1.000mol/1]XIANGDANGDEYIKEBIAOSHIDETIEDEZHILIANG; mWEISHILIAODEZHILIANGDESHUZHI。

澳门网上葡京真人4.1FANGFATIYAO4YANJIDU

ZAISHIYANGZHONGJIARUDINGLIANGYANSUANRONGYE,ZAIJIALVHUAJIAYANQIAOTIE,RANHOUYIQINGYANGHUANABIAOZHUNDIDINGCAYECHENGQU500gFUHUAJIA,YI200mlBUHANERYANGHUATANDEZHENGLIUSHUIRONGJIEHOU,XISHIDAO1000ml,JIARU2mFENGANZHISHIJIBINGYONGQINGYANGHUANARONGYEHUOYANSUANRONGYEDIAOJIERONGYEZHIWEIHONGSE,LVQUBURONGWUHOUZHUCUNYUSULIAOPINGZHONG。4.2.5YANGHUAJIARONGYE: 500g/L.CHENGQUYUE(1.5±0.001)gWUYANG,ZHIYU250mlZHUIXINGPINGZHONG,YONGYIYEGUANZHUNQUEJIARU25.00mlYANSUANRONGYE,JIA20mlZHUFEIHOUDEZHENGLIUSHUI,YAOYUN,GAISHANGBIAOMIANm。ZAISHIWENXIAFANGZHI10min,ZAIJIARULVHUAJIARONGYE10ml,YAOYUN,JIA5DIFENSANZHISHIJI,LIJIYONGQINGYANGHUANABIAOZHUNDIDINGRONGYEDIDINGZHIDANHONGSE(35BUTUN)WEIZHONGDIAN,TONGSHIYONGZHUFEIHOULENGQUEDEZHENGLIUSHUIDAITISHIYANGZUOKONGBAISHIYAN。

4.4JIEGUODEBIAOSHU

YANJIDUHANLIANGYIZHILIANGFENSHUWsJIt,SHUZHIYI%BIAOSHI,ANSHI(8)JISUAN:WS (%) = (V-Vo) exO. 0170/17.0 X100QIANWA,/18.62SHIZHONG, cWEIQINGYANGHUANABIAOZHUNDIDINGRONGYENONGDUDEZHUNQUESHUZHI, mol/L: VWEIDIDINGSHIXIAOHAOQINGYANGHUANABIAOZHUNDIDINGRONGYEDETIJIDESHUZHI, ml; V。WEIDIDINGKONGBAISHIXIAOHAOQINGYANGHUANABIAOZHUNDIDINGRONGYEDETIJIDESHUZHI, mls 0. 0170WEIYU1.00mlQINGYANGHUANABIAOZHUNDIDINGRONGYE[e(NaOH) = 1.000mo/A])XIANGDANGDEYIKEBIAOSHIDEQIANGJI(OH-)DEZHILIANG; 18.62WEITIEDEMOERZHILIANG(1/3Fe),g/mol; WEISHIYANGZHONGSANJIATIEDEZHILIANGBAIFENSHU, w,-w,-wsHUOW,=w2-w3; mWEISHILIAODEZHILIANGDESHUZHI,g.ZHONGYEXUANXIN1r0DEWANG4HAICHENGQU1.0gSHIYANG,ZHIYUSHAOBEIZHONG,YONGSHUIXISHI,QUANBUZHUANYIZHI100mlRONGLIANGPINGZHONGXISHIZHIKEDU。YONGpH=4.00DELINBENERJIASUANQINGJIAHUANCHONGRONGYEHEpH=6.86DELINSUANERQINGJIALINBENERJIASUANQINGJIAHUANCHONGRONGYEDINGWEIHOU,JIANGSHIYANGRONGYEDAORUSHAOBEI,JIANGBAOHEGANGONGDIANJIHEBOLIDIANJIJINRENBEICERONGYEZHONG,ZHIpHZHIWENDINGSHI(1minNEIpHZHIDEBIANHUABUDAYU0.1)DUSHU。

6.1 SHIJIHECAILIAO

SMAXINrHE0SHEoCHIDENGFA)BAODE,mGAOLINGERFANGZHONGZHONGWEIXIANGBUYANSUANRONGYE1+49,3tmHeeDUIYANGLIUCI,XUMEIWUaFAZHUDIDEeHUZHENGPINGHEYUGANZAOJIEJINGDECHENGLIANGPINGZHONGCHENGQUYUE20g 1XINGSHIYANG,HUO10g 1IXINGSHIYANG,JINGQUEZHI0.001g,YIREN250mlSHAOBEIZHONG。DUI1XINGSHIYANG,YONGSHUIFENCIXIDICHENGLIANGPING,XIYEBINGRUSHENGSHIYANGDESHAOBEIZHONG,JIASHUIZHIYUE100ml,JIAOBANJUNYUN;DUI1XINGSHIYANG,YONGYANSUANRONGYEFENCIXIDICHENGLIANGPING,XIYEBINGRUSHENGSHIYANGDESHAOBEIZHONG,JIAYANSUANRONGYEZHIZONGTIJIYUE100ml,JIAOBANRONGJIE,ZAI50~55℃SHUIYUZHONGBAOWEN15min,YONGYIYU105110℃GANZAOZHIHENGZHONGDEGANTASHIGUOLVQICHOULV,YONGSHUIXIDICANZHAZHILVYEZHONGBUHANLVLIZI(YONGXIAOSUANYINRONGYEJIANCHA),BAZENGJIEFANGRUDIANREHENGWENGANZAOXIANGNEI,YU105~110℃XIAHONGZHIHENGZHONG。

6.4 JIEGUODEBIAOSHU

不溶物含量以质量分数Woit,数值以%表示,米式中,m为坩埚式过滤器连同残渣的质量的数值, g: m2为坩塌式过滤器的质量的数值, gim为试料的质量的数值。本内容由巩义恒信达原创,欢迎转载,转载需注明出处http://yiwuqipai.com        KP20191016HXD01


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巩义市恒信达环保科技有限公司澳门网上葡京真人-销售部电话:0371-63263169 手机:赵-19939951369;康-13027510201;地址:河南省巩义市北山口镇常庄村-水处理产业聚集区